For Holograms recorded with continuous laser
Exposure:
Plate may be exposed directly after being removed from the box (after a
stabilization period of 30 minutes at ambient room temperature, if
the plate was just removed from refrigeration). For any given
laser-power, the exposure time must be precisely adjusted, this is
the ONLY parameter that can or should be adjusted for perfect
holograms. See the curve
above to understand better. For a given emulsion and laser set
up, you must find the correct exposure through experiment. Extremely bright images, totally noise free, with more
than 90% diffraction efficiency, can be
obtained with ULTIMATE plates in almost any recording set up, if
you use the correct exposure time.
Safe Developer: We
have adjusted our custom developers for the special emulsions we supply.
It is a fine grain developer, totally safe to use, delivered as a
concentrate.
For 4"x5" plates
and film: just before use take 5cc
from the concentrate bottle and add 50ml water (Ultimate 15nm
and Ultimate 8nm). For a 30x40cm, take 40ml plus 400ml water.
After processing, we recommend disposing of this diluted
developer although some users have reported that it may be can re-used within 6
hours: please test this if you'd like and let us know your
results.
Processing time: 6 minutes @ 20°C for Ultimate-15 and 8 minutes
@ 20°C for Ultimate-08 .
Development generally starts after 20-30 seconds with new
plates (plates used prior to the stated "use after" date) or immediatly with plates
used after the "use after" date. It gives a reddish color
on the plate for Ultimate 15nm , and pale yellow/orange color
with Ultimate 08nm, due to the very small grain size (Mie
diffusion). This is very likely much smaller than any emulsion you've
used before. It is normal that you get NO DENSITY at all (for
08nm) or can not increase the density to dark black like on old
Agfa material (for 15nm), so do not expose or try to process
more. After this recommended development time, you can be sure that all
exposed grains are processed. There is no possible density
control in this step (comparing to standard photofilm or current
larger-grained holographic plates like AGFA, etc.) that is why the
exposure time is THE ONLY VARIABLE PARAMETER.
Important
Notice: an
unexposed area can blacken in the developer. As the exposed area
blackens very little due to the fine grain, it seems the
unexposed and exposed parts have the same color. This is a
normal characteristic of our material (15nm). It does not mean
the material is fogged at all. When bleaching, the unexposed
part (which is in fact only "colored") it will become totally
transparent when the exposed area is slightly milky. This is
totally visible when the plate is dried.
Rinse:
tap water 30 seconds.
Safe Bleach:
with
continuous slow agitation, to obtain good transparency
(about 3 or 4 minutes ). Then let the plate sit for about the
same time in this bath until complete transparency. The plate
must be completely transparent like glass. If the plate looks
milky, you are overexposed
Rinse:
tap water for 2 minutes
Drying:
solution 1 :No contact natural drying. No contact
is made with the emulsion.
step 1: Rinse 1
minute in distilled or demineralized water with a few drops of
Kodak fotoflo
step 2: Let it dry
supported vertically for a few minutes (other solution
without contact: alcohol (ethanol) 50% 2 minutes; 100% for 2
minutes)
solution 2 :
fast drying but be careful not to scratch the emulsion.
step 1: Rinse 1
minute in distilled or demineralized water a few drops of
fotoflo (Kodak)
step 2: squeegee
the film/plate and fast dry it with hair dryer
PROCESSING FOR
ULTIMATE LIPPMANN:
There are initial
recommendations based on our experimental experience at this
time
Lumiere developer: For processing one 4x5" film/plate:
mix just before use : part A 0,1g pyrogallol in 50ml water +
part B ,0,75ml ammonia solution + 1g KBr in 50ml water
The standard developer for holography could work well too:
processing 6 minutes dilluted 1+10. the color is extremly pale
yellow. Wash and dry. (no bleach after developer)
A little swell of
the emulsion has to be done for perfect color reconstruction
after developer. No bleaching has to be done. The swelling can
be done with a sorbitol solution (5-10%)